dc.contributor.author |
Remani, K C |
|
dc.contributor.author |
Ghosh, S |
|
dc.date.accessioned |
2016-12-08T05:59:57Z |
|
dc.date.available |
2016-12-08T05:59:57Z |
|
dc.date.issued |
2009-10 |
|
dc.identifier.citation |
Transactions of the Indian Ceramic Society, 68(4):185-188 |
en_US |
dc.identifier.uri |
http://hdl.handle.net/123456789/2544 |
|
dc.description.abstract |
Uniform nanosized 3–6 nm cerium oxide single crystals have been synthesized by ammonia precipitation in alcohol-water mixed solvent. The size was estimated by photon correlation spectroscopy (PCS), X-ray diffraction (XRD) and high resolution transmission electron microscopy (HR-TEM). The surface area of CeO2 nanocrystals were measured by Brunauer-Emmett-Teller (BET) technique. The nanoparticles synthesized were mono-dispersed with a narrow size distribution with low polydispersity index (PDI). The size of the ceria nanocrystals synthesized was found to decrease with decrease in the ϵ of the solvent. The crystals precipitated from isopropyl alcohol were highly crystalline. The smallest CeO2 crystals were obtained using ethylene glycol/water medium whereas lowest PDI was obtained from IPA/water system. |
en_US |
dc.language.iso |
en |
en_US |
dc.publisher |
The Indian Ceramic Society |
en_US |
dc.subject |
CeO2 |
en_US |
dc.subject |
Nanocrystals |
en_US |
dc.subject |
Precipitation |
en_US |
dc.subject |
Mixed solvent |
en_US |
dc.subject |
HR-TEM |
en_US |
dc.title |
Nanocrystalline Ceria through Homogeneous Precipitation in Alcohol-Water Mixed Solvent |
en_US |
dc.type |
Article |
en_US |